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<title>UTas ePrints - Bis[tris(pyridin-2-yl)methanol-K2N,N']palladium(II) dinitrate at 150 and 298 K</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Skelton, B.W." name="eprints.creators_name" />
<meta content="Traill, P.R." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
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<meta content="The title complex, [Pd{(py)3COH}2](NO3)2, where (py)3COH is tris(pyridin-2-yl)methanol (C16H13N3O), studied at 150 and 298 K, has the potentially tridentate ligands present as bidentate ligands, with the Pd atom at a centre of symmetry. At 150 K, the PdÐN distances are 2.022 (3) and 2.026 (3) A. The mean planes of the coordinated pyridine groups form dihedral angles of 42.1 (1) and 45.3 (1) degrees (at 150 K) with the coordination plane; the uncoordinated rings situated either side of the coordination plane form dihedral angles of 42.2 (1)degrees with it. The nitrate ions are regular and interact weakly with the hydroxyl group." name="eprints.abstract" />
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B. W. & White, A. H. (1994). J. Organomet. Chem. 471, C8±10.
Canty, A. J., Minchin, N. J., Engelhardt, L. M., Skelton, B. W. & White, A. H.
(1986). J. Chem. Soc. Dalton Trans. pp. 645±650.
Enraf±Nonius (1989). CAD-4 Software. Enraf±Nonius, Delft, The Netherlands.
Hall, S. R., King, G. S. D. & Stewart, J. M. (1995). The Xtal3.5 User's Manual.
University of Western Australia: Lamb, Perth.
Sheldrick, G. M. (1996). SADABS. University of GoÈ ttingen, Germany.
Siemens (1995). SMART and SAINT. Versions 4.0. Siemens Analytical X-ray
Instruments Inc., Madison, Wisconsin, USA.
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<meta content="Canty, A.J. and Skelton, B.W. and Traill, P.R. and White, A.H. (2004) Bis[tris(pyridin-2-yl)methanol-K2N,N']palladium(II) dinitrate at 150 and 298 K. Acta Crystallographica Section C, C60 (part 7). m305-m307. ISSN 0108-2701" name="eprints.citation" />
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<meta content="The title complex, [Pd{(py)3COH}2](NO3)2, where (py)3COH is tris(pyridin-2-yl)methanol (C16H13N3O), studied at 150 and 298 K, has the potentially tridentate ligands present as bidentate ligands, with the Pd atom at a centre of symmetry. At 150 K, the PdÐN distances are 2.022 (3) and 2.026 (3) A. The mean planes of the coordinated pyridine groups form dihedral angles of 42.1 (1) and 45.3 (1) degrees (at 150 K) with the coordination plane; the uncoordinated rings situated either side of the coordination plane form dihedral angles of 42.2 (1)degrees with it. The nitrate ions are regular and interact weakly with the hydroxyl group." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Bis[tris(pyridin-2-yl)methanol-K2N,N']palladium(II) dinitrate at 150 and 298 K</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">Traill, P.R.</span> and <span class="person_name">White, A.H.</span> (2004) <xhtml:em>Bis[tris(pyridin-2-yl)methanol-K2N,N']palladium(II) dinitrate at 150 and 298 K.</xhtml:em> Acta Crystallographica Section C, C60 (part 7). m305-m307. ISSN 0108-2701</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2787/1/AC2C_C602C_m305.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2787/1/AC2C_C602C_m305.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />266Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="3755" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1107/S0108270104010893">http://dx.doi.org/10.1107/S0108270104010893</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The title complex, [Pd{(py)3COH}2](NO3)2, where (py)3COH is tris(pyridin-2-yl)methanol (C16H13N3O), studied at 150 and 298 K, has the potentially tridentate ligands present as bidentate ligands, with the Pd atom at a centre of symmetry. At 150 K, the PdÐN distances are 2.022 (3) and 2.026 (3) A. The mean planes of the coordinated pyridine groups form dihedral angles of 42.1 (1) and 45.3 (1) degrees (at 150 K) with the coordination plane; the uncoordinated rings situated either side of the coordination plane form dihedral angles of 42.2 (1)degrees with it. The nitrate ions are regular and interact weakly with the hydroxyl group.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Additional Information:</th><td valign="top" class="ep_row">"The definitive version is available at www.blackwell-synergy.com"
</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250201.html">250000 Chemical Sciences > 250200 Inorganic Chemistry > 250201 Transition Metal Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2787</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">02 Jan 2008 14:05</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">01 Feb 2008 14:15</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2787;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2787">item control page</a></p>
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